FT-NIR Spectrometer

The FT-NIR: fibered NIR spectrometer with a spectral range from 900 to 2600 nm

If you are looking for a high performance, compact and affordable NIR spectrometer, the ARCoptix FT-NIR Rocket is the instrument that you need. Thanks to its permanently aligned interferometer and solid-state reference laser, the FT-NIR Rocket offers excellent stability in both intensity and wavelength scales. The FT-NIR Rocket is compatible with light sources and sampling accessories (like fibers, cuvette folder, ...) typically used with array-detector based NIR spectrometers.

The FT-NIR Rocket is a high-performance system combining high resolution, broad wavelength range and excellent sensitivity. FT-NIR functioning principle permits to measure over a much broader range than grating spectrometers that are limited to 2100nm. Its outstanding stability in both wavelength and intensity scales makes it an ideal tool for highly reproducible chemometric analysis. In comparison to array-photodiode NIR spectrometers, the single photodiode operation of the FT-NIR ensures no defect pixels, no gain variation among pixels and no dark-current drifts. Also, the device does not suffer from stray-light as grating spectrometers. Finally, all these advantages come at a very attractive pricing!

Due to its functioning principle the FT-NIR is superior to any grating spectrometer on the market!

ARCoptix also proposes a Mid-IR version of the FT Rocket with spectral ranges of 2-6 or 2-12μm.

PRICE starting at 15'400 EUR (900-2600 nm inclusive software)

Wide wavelength range 0.9-2.6μm
High resolution 4cm^-1
(equivalent to <0.5nm@1um and <2.5nm@2.5um)
Excellent stability in intensity & wavelength scale (no dark current-induced drift, internal reference laser)

Very good sensitivity (available with 2TE cooled InGaAs)

Compact and rugger, easy-to-use fiber input system
Cost effective (single NIR photodiode)

How does it work?

Permanentely aligned interferometer

The heart of the FT-Rocket is dual corner-cube (retro-reflector) interferometer. The two corner-cubes are solidary to a common swinging arm, which rotates to create an optical path difference in the two arms of the interferometer.
This type of design is called a permanently aligned interferometer, as the alignment of the system is known to be the most robust against vibrations and temperature drifts. It never has to be realigned.
The swinging arm of the interferometer rotates on wear-free flexure system, making this mechanical system extremely robust and durable.

Solid-state reference laser

For measuring the movement of the mirrors, a solid-state reference laser is coupled into the interferometer. Compared to classic HeNe lasers, the solid-state lasers that we use are more compact and have a much longer life-time. They have a very low temperature-induced wavelegnth drift and, when kept at constant temperature with a Peltier element, their wavelength can be stabilized to a few PPM, thus providing a very accurate and reproducible wavelength scale. This is crucial for ensuring a day-to-day and unit-to-unit consistency..

Specifications

Model	FT-NIR 0.9-2.6
Type of interferometer	Permanentely aligned, double retro-reflector design
Spectral range [cm^-1]	3800 - 11000
Spectral range [nm]	900 - 2600
Spectral resolution in wavenumber:	4cm^-1
SNR (8cm-1 resolution, 1 minute scan time)	>200'000:1
Long term baseline intensity stability	< 2% (1100-2500nm) over 10 hours
Wave-number repetability	< 10ppm
Detector	Extended type InGaAs PIN photodiode, optionally 2TE cooled
Effective measurement time	1 spectrum / second in continuous mode aquisition
Optical fiber connector	SMA 905
Optical entrance	< 1mm (fiber core diameter) NA=0.25
Reference laser	Solid-state 795nm, temperature stabilized.
A/D converter	24 bit
Power requirements	7.5 - 12V / 1-6W depending on versions
Operating temperature	5°C-40°C
Communication interface	USB 2.0 (optionally Ethernet)
Software interface	Windows 7 & 10 API for controlling the instrument via our DLL
Dimensions	180mm x 160mm x 80mm
Weight	1700g

FAQ

What is the resolution of the FT-NIR Rocket in nm (wavelengths)?

The resolution of Fourier-transform spectrometers is usually expressed in wave-numbers (ν), which are simply the inverse of wavelength (ν=1/λ). The conversion betwen wave-number resolution and wavelength resolution is Δλ = λ² · Δν. The the graph below shows this conversion for the situations where Δν = 8cm^-1 (standard setting of the ARCoptix FT-NIR 0.9-2.6) or Δν = 4cm^-1(optional higher resolution).

Can I use the FT-NIR Rocket with standard fiber-optics accessories?

Yes. Although the ARCoptix FT-NIR is not a dispersive but a Fourier-transform spectrometer, accessories normally used with dispersive spectrometer are compatible. The spectrometer has a SMA-905 input fiber connector. One just has to take care that accessories are NIR compatible. For example, optical fibers must be rated "low-OH content" to avoid too high absorption in the NIR.

What is the temperature-stabilized internal reference laser?

The precision of the wavelength scale in Fourier-transform spectrometers relies on its internal reference laser. In our compact FT spectrometers, the reference laser is a solid-state type whose central wavelength has a naturally low temperature-induced drift, ~70 ppm/ºC. In some applications, this is sufficient. But in other applications, a more reproducible wavelength scale must be achieved by the spectrometer. With the temperature-stabilization of the laser (via a thermoelectric element) a wavelength reproducibility < 10 ppm can be guaranteed all over the instrument operational temperature range (5-40 ºC). To give an example, at 1000nm wavelength, a shift of 10 ppm means 10E-6 * 1000nm = 0.01nm. This is especially important for applications such as laser characterization or chemometric analysis.

Are thermoelectrically (TE) cooled detectors available on the FT-NIR?

Yes, we can optionally install 1-TE or 2-TE InGaAs detectors on our FT-NIR spectrometer. This provides an advantage in situations where weak light signals have to be detected. The 1-TE cooler lowers the minimum detectable power by a factor of 2-3, and the 2-TE cooler by a factor of 4-5 with respect to an uncooled detector.

Free GUI basic software

The FTIR Rocket is delivered with a free Windows 7 & Windows 10 compatible graphical user interface (GUI) program.

The free basic software package allows the user to:

Configure hardware measurement parameters (amplifier gain, averaging, ...).
Display real-time spectral measurement results.
Set reference spectra (white, dark) and choose among raw spectra, transmission or reflection mode.
Perform usual operations such as save, open, zoom, rescale...
Select features specific to Fourier transform spectrometry: choose among spectrum or interferogram averaging, apodization, look and save the interferograms, etc.

Free API & Examples

The FTIR Rocket is also delivered with a free API that allows you to control the spectrometer with custom code via our DLLs. Examples are available for the following languages:

C++
C#
Labview
Matlab

Advanced data processing & analysis software

In collaboration with Labcognition GmbH in Germany we also offer additional Panorama software packages:

Math Add-on module

contains a set of standard manipulation operations used in spectroscopy, like normalization, derivative, baseline correction, peak picking and more. In addition some special operations are available, like multiplicative scatter correction, thickness correction or standard normal variate correction and others.

Quantity Add-on module

is an expert in multivariate data analysis with quantitative methods like PLS and MLR. A convenient and intuitive wizard guides you through all steps of calibration model development. Complex statistical methods become very easy to use even for non-experienced users.

Search Add-on module

is an ideal add-on to archive your spectroscopic data and related information. It includes spectrum and full text search functionality on spectral libraries of various different library formats or directly on data in the file system.

IRAnalyze software package

is a highly sophisticated IR spectrum interpretation tool. Based on an IR spectrum, it provides you with automatic results for IR bands to functional group correlations and their characteristic frequencies. Furthermore, it is a comprehensive electronic dictionary to browse frequiencies for correlated IR bands.

Accessories

Transmission measurement

The sketch below shows a typical configuration for using the FT-NIR Rocket for transmission measurements. In addition to the spectrometer, you will need one NIR light source, a cuvette/sample holder and 2 NIR optical fibers.

ArcLight NIR lamps

The ARCoptix ArcLight NIR is the version of our lamp optimized for the VIS-NIR (400 – 4,000nm) spectral range. It uses a high temperature (>2850 K) and is available in versions from 5 to 20W. The lamp has a removable fiber coupler SMA-905 connector.

DOWNLOAD Datasheet of ArcLight Lamps

Cuvette / sample holder (CUV-NIR)

The CUV-NIR is a cuvette holder ideal for the visible to near-infrared (0.4-2.6 microns). It comes with 2 fiber collimators / fiber couplers with SMA-905 connectors. The sample slot is 12.5mm wide, thus accepting glass cuvettes with an optical path of up to 10mm. The CUV-NIR has an additional slot to hold a filter, e.g to reduce heating of the sample and shot noise due to light out of the spectral range of interest.

Diffuse reflection measurement

Another typical measurement configuration is diffuse reflectance. There are several possible configurations, among which a very good one is to use our internally illuminated integrating sphere, as shown in the illustration below.

Integrating sphere with internal light source (ArcSphere-50-Hal)

The ArcSphere-50-Hal is an integrating sphere with internal halogen light source for diffuse reflection VIS/NIR measurements. The ArcSphere-50-Hal has an internal
diameter of 50mm, a sample port diameter of 10mm, and an SMA-905 fiber connector to connect to the spectrometer.
The internally illuminated integrating sphere provides a much stronger signal than spheres illuminated via fiber optic coupled.

DOWNLOAD Datasheet ArcSphere-50-Hal

Non-exclusive Distributor list for spectrometers:

For OEM Business: contact Arcoptix directly.
France, Germany Italy, UK
France
Spain
Benelux
USA	MADISON INSTRUMENTS
Russia, Moscow
Japan
Singapore
China
Australia
South Korea
Taiwan
Poland
Switzerland and Rest of the world